Separation Process Engineering
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Profiles for Binary Distillation 4. Open Steam Heating 4. Other Distillation Column Situations 4. Limiting Operating Conditions 4. Efficiencies 4. Simulation Problems 4. New Uses for Old Columns 4. Subcooled Reflux and Superheated Boilup 4. Comparisons between Analytical and Graphical Methods 4. Calculational Difficulties 5. Profiles for Multicomponent Distillation 5.
Summary-Objectives References Homework Appendix.
Introduction to Matrix Solution for Multicomponent Distillation 6. Component Mass Balances in Matrix Form 6. Initial Guesses for Flow Rates and Temperatures 6. Temperature Convergence 6. Energy Balances in Matrix Form 6. Discussion 6. Total Reflux: Fenske Equation 7.
Minimum Reflux: Underwood Equations 7. Breaking Azeotropes with Other Separators 8.
Separation Process Engineering 4th edition | , | VitalSource
Binary Heterogeneous Azeotropic Distillation Processes 8. Steam Distillation 8.
Two-Pressure Distillation Processes 8. Complex Ternary Distillation Systems 8. Extractive Distillation 8. Azeotropic Distillation with Added Solvent 8. Distillation with Chemical Reaction 8. Binary Batch Distillation: Rayleigh Equation 9. Simple Binary Batch Distillation 9. Constant-Level Batch Distillation 9.
Batch Steam Distillation 9. Multistage Batch Distillation 9. Operating Time 9. Staged Column Equipment Description Tray Efficiencies Column Diameter Calculations Balancing Calculated Diameters Sieve Tray Layout and Tray Hydraulics Valve Tray Design Introduction to Packed Column Design Packed Column Internals Packed Column Flooding and Diameter Calculation Economic Trade-Offs for Packed Columns Choice of Column Type Distillation Costs Operating Effects on Costs Changes in Plant Operating Rates Energy Conservation in Distillation Absorption and Stripping Equilibria Stripping Analysis for Dilute Systems Efficiencies Column Diameter Dilute Multisolute Absorbers and Strippers Matrix Solution for Concentrated Absorbers and Strippers Irreversible Absorption and Co-Current Cascades Extraction Processes and Equipment Countercurrent Extraction Dilute Fractional Extraction Concentrated Immiscible Extraction Immiscible Batch Extraction Mixing Calculations and the Lever-Arm Rule Extraction Computer Simulations Design of Mixer-Settlers Washing Leaching with Constant Flow Rates Leaching with Variable Flow Rates Supercritical Fluid Extraction Application to Other Separations Molecular Movement Leads to Mass Transfer Fickian Model of Diffusivity Values and Correlations for Fickian Binary Diffusivities This work is protected by United States copyright laws and is provided solely for the use of instructors in teaching their courses and assessing student learning.
Dissemination or sale of any part of this work including on the World Wide Web will destroy the integrity of the work and is not permitted.
Separation Process Engineering
The work and materials from it should never be made available to students except by instructors using the accompanying text in their classes. All recipients of this work are expected to abide by these restrictions and to honor the intended pedagogical purposes and the needs of other instructors who rely on these materials. Wankat 4. Note that the answers for graphical solutions can vary depending upon the accuracy of the draftsperson; however, the methods shown here should be correct. Although every effort has been made to ensure that solutions are correct, there will be errors.
Please inform the author of errors wankat purdue. The assistance of Mrs. Karen Heide in preparing this Solutions Manual is gratefully acknowledged. This Solutions Manual is provided as a service to professors who adopt the book Separation Process Engineering, Third Edition, in their courses. It is copyrighted and is not to be distributed or sold. No parts of this manual should be placed on the Internet without explicit written consent from the author.
Learning requires practice and feedback, not mere copying. Unfortunately, there are students and other people who do not realize that students do not learn if they copy solutions from a solutions manual. Some of these people are willing to put illegal copies of solution manuals on the Internet either for profit or for free. These illegal copies reduce student learning and make it more difficult for professors to teach courses. To aid everyone involved in teaching and learning separation processes, please help protect the integrity of the Solutions Manual.
Wankat 5. Wankat E-mail: wankat purdue. Use e-mail to communicate with Prof. Wankat for help. These times are reserved for students. On Wednesdays I will be in the computer lab from to P. Other times by appointment only. You are unlikely to find me if you drop in at a time other than office hours without an appointment.
TA's — Office hours will be M to , T to and W to starting second week of semester. Goals: By the end of CHE you should be able to: 1.
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Design flash distillation by hand and computer calculations; 2. Design distillation systems by hand and computer calculations; 3. Design absorbers and strippers by hand and computer calculations; 4. Design extraction systems by hand and computer calculations; 5. Design membrane separation systems. Distillation is the most important separation method in the chemical and petroleum industries. Separations are one of the key items which delineate chemical engineering from the other engineering disciplines.
Course The basic course outline is: Structure: 1. Introductory Material 1 week 2.
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Flash Distillation 1 week 3. Binary Distillation 2 weeks 4. Multicomponent Distillation 2 weeks 5. Complex Distillation 2 weeks 6. Batch Distillation 1 week 7. Distillation Design 1 week 8. Extraction 1 week Membrane separations 2 weeks The detailed course outline is attached. The typical weekly schedule will be: 7. Suggested Read book before class.
Come to class prepared. There will be Study short quizzes to encourage preparation. New material Procedure: will be presented in class as needed. Material in the book that is a review or is easy to understand will not be lectured on. Ask questions if the book is not clear. After class, reread the book. Make extensive notes on or in the book.